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Title: Dicyclohexylbis(naphthalen-1-ylmethyl)phosphonium chloride chloroform disolvate
Authors: Gowrisankar, S.Neumann, H.Spannenberg, A.Beller, M.
Publishers Version: https://doi.org/10.1107/S1600536812046661
Issue Date: 2012
Published in: Acta Crystallographica Section E: Structure Reports Online Vol. 68 (2012), No. 12
Publisher: Chester : International Union of Crystallography
Abstract: In the title solvated phosphonium salt, C34H40P+·Cl -·2CHCl3, the two cyclohexyl and two 1-naphthylmethyl groups at the P atom are in a distorted tetrahedral arrangement [105.26 (6)-113.35 (6)°]. Both cyclohexyl rings adopt a chair conformation. The dihedral angle between the naphthyl ring systems is 74.08 (3)°.
Keywords: data-to-parameter ratio = 22.3; mean ω(C-C) = 0.002 Å; R factor = 0.030; single-crystal X-ray study; T = 150 K; wR factor = 0.080
DDC: 540
License: CC BY 4.0 Unported
Link to License: https://creativecommons.org/licenses/by/4.0/
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